Catalytic Cross-Coupling of Vinyl Golds with Diazonium Salts under Photoredox and Thermal Conditions

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초록

Catalytically generated vinyl gold complexes from tert-butyl allenoates were found to undergo an efficient cross-coupling with arenediazonium salts. The gold(I)-gold(III) redox cycle can be accessed under two different conditions, i.e., visible-light photoredox as well as a thermally induced radical chain pathway. The current C(sp(2))-C(sp(2)) cross-coupling protocol that is catalytic in gold, would make available desirable structural diversity to the traditional cross-coupling chemistry.

키워드

cross-couplingdiazonium saltsgold catalysisradical chain reactionvisible light photocatalysisC-H ARYLATIONVISIBLE-LIGHTSTRUCTURAL-CHARACTERIZATIONARENEDIAZONIUM SALTSNONACTIVATED ARENESCATIONIC GOLD(I)ROOM-TEMPERATUREALKENESCYCLIZATIONCOMPLEXES
제목
Catalytic Cross-Coupling of Vinyl Golds with Diazonium Salts under Photoredox and Thermal Conditions
저자
Patil, Dilip V.Yun, HokeunShin, Senghoon
DOI
10.1002/adsc.201500525
발행일
2015-08
유형
Article
저널명
Journal für Praktische Chemie
357
12
페이지
2622 ~ 2628