Intramolecular Cyclization of 2-Alkynylphenylcarbonyls With a Pendant Double Bond under Copper Catalysis: A General Approach to Norabietane Core Structure

  • Kang, Juyeon
  • Lee, Ju Hui
  • Lee, Junseong
  • Oh, Chang Ho
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초록

Synthetic routes leading to [6,6,6]-tricyclic compounds were reported using metal catalysts from ene-yne-aldehydes in our group. Based on this result, the synthesis of various [6,6,6]-tricyclic compounds is reported using transition metal-catalyzed cyclization from enyne-carbonyl substrates containing H, Me, Ph, OMe, CO2Me, and CO(2)i-Pr groups. Tricyclic compounds containing the CO2Me group would be the prospective precursors of the natural product Lepenine.

키워드

[666]-tricyclic compoundcopper catalystcycloisomerizationenyne-carbonylLepenine precursorDITERPENOID ALKALOIDSGOLDDERIVATIVESCYCLOADDITIONPHENANTHRENESANNULATIONENYNALSROUTE
제목
Intramolecular Cyclization of 2-Alkynylphenylcarbonyls With a Pendant Double Bond under Copper Catalysis: A General Approach to Norabietane Core Structure
저자
Kang, JuyeonLee, Ju HuiLee, JunseongOh, Chang Ho
DOI
10.1002/ajoc.202200244
발행일
2022-07
유형
Article; Early Access
저널명
Asian Journal of Organic Chemistry
11
7
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